Advanced three-dimensional electron microscopy techniques in the quest for better structural and functional materials
(2013) Science and Technology of Advanced Materials — Vol. 14, p. 14206 (2013)
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- Abstract
- After a short review of electron tomography techniques for materials science, this overview will cover some recent results on different shape memory and nanostructured metallic systems obtained by various three-dimensional (3D) electron imaging techniques. In binary Ni–Ti, the 3D morphology and distribution of Ni4Ti3 precipitates are investigated by using FIB/SEM slice-and-view yielding 3D data stacks. Different quantification techniques will be presented including the principal ellipsoid for a given precipitate, shape classification following a Zingg scheme, particle distribution function, distance transform and water penetration. The latter is a novel approach to quantifying the expected matrix transformation in between the precipitates. The different samples investigated include a single crystal annealed with and without compression yielding layered and autocatalytic precipitation, respectively, and a polycrystal revealing different densities and sizes of the precipitates resulting in a multistage transformation process. Electron tomography was used to understand the interaction between focused ion beam-induced Frank loops and long dislocation structures in nanobeams of Al exhibiting special mechanical behaviour measured by on-chip deposition. Atomic resolution electron tomography is demonstrated on Ag nanoparticles in an Al matrix.
- Affiliations
University of Antwerp EMAT
Citations
Schryvers, D., Cao, S., Tirry, W., Idrissi, H., & Van Aert, S. (2013). Advanced three-dimensional electron microscopy techniques in the quest for better structural and functional materials. Science and Technology of Advanced Materials, 14, 14206. https://doi.org/10.1088/1468-6996/14/1/014206 (Original work published 2013)