Synthesis and Characterization of (z)-1-[2-(triarylstannyl)vinyl]-cyclo-hexanols and Their Arylhalostannyl Derivatives
(1994) Zeitschrift für anorganische und allgemeine Chemie — Vol. 620, n° 6, p. 1006-1010 (1994)
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- 1-Ethynyl-1-cyclohexanol reacts with a triaryltin hydride Ar3SnH (Ar = phenyl, p-tolyl) and generates the corresponding (Z)-1-[2-(triarylstannyl)vinyl]-1-cyclohexanol. The product obtained reacts with one or two equivalents of halogen (ICl or I2) to form the associated (Z)-1-[2-(diarylhalostannyl)-vinyl]-1-cyclohexanol or (Z)-1-[2-(aryldihalostannyl)vinyl]-1-cyclohexanol, respectively. All compounds were characterized by elemental analysis, H-1, C-13, Sn-119 NMR and Mossbauer spectroscopy.
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Xin, FF., Lin, SX., Jie, FY., Pan, H., Gielen, M., Kayser, F., & Willem, R. (1994). Synthesis and Characterization of (z)-1-[2-(triarylstannyl)vinyl]-cyclo-hexanols and Their Arylhalostannyl Derivatives. Zeitschrift für anorganische und allgemeine Chemie, 620(6), 1006-1010. https://doi.org/10.1002/zaac.19946200609 (Original work published 1994)