Crystal structure of N-[1',1'-(diphenyl)-hydroxymethyl]-3(S)-[1'(R)hydroxyethyl]-4(S)-(t-butyl-oxomethyl)-azetidin-2-one, C23H27NO4, an unexpectedly stable intermediate in the photochemical cleavage of N-benzhydryl protecting group

Tinant, Bernard;Laurent, Marie-Alexandre;Cérésiat, Marcel;Marchand-Brynaert, Jacqueline
(2003) Zeitschrift fuer Kristallographie - New Crystal Structures — Vol. 218, n° 1, p. 145-147 (2003)

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  • Tinant, BernardUCLouvain
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  • Laurent, Marie-AlexandreUCLouvain
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  • Cérésiat, Marcel
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  • Marchand-Brynaert, JacquelineUCLouvain
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Abstract
C23H27NO4, monoclinic, P12(1)1 (No. 4), a = 6.356(2) Angstrom, b = 17.418(5)Angstrom, c = 9.586(3)Angstrom, beta = 100.75(2)degrees, V = 1042.6 Angstrom(3), Z = 2, R-gt(F) = 0.055, wR(ref)(F) = 0.153, T = 293 K.
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Tinant, B., Laurent, M.-A., Cérésiat, M., & Marchand-Brynaert, J. (2003). Crystal structure of N-[1′,1′-(diphenyl)-hydroxymethyl]-3(S)-[1′(R)hydroxyethyl]-4(S)-(t-butyl-oxomethyl)-azetidin-2-one, C23H27NO4, an unexpectedly stable intermediate in the photochemical cleavage of N-benzhydryl protecting group. Zeitschrift fuer Kristallographie - New Crystal Structures, 218(1), 145-147. https://hdl.handle.net/2078.5/73797 (Original work published 2003)