Efficient syntheses of the polyene fragments present in amphidinols

Cossy, Janine;Tsuchiya, Tomoki;Ferrie, Laurent;Reymond, Sebastien;Marko, Istvan;et.al.
(2007) Synlett : accounts and rapid communications in synthetic organic chemistry — n° 14, p. 2286-2288 (2007)

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  • Cossy, Janine
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  • Tsuchiya, Tomoki
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  • Ferrie, Laurent
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  • Reymond, Sebastien
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  • Jourdain, PierreUCLouvain
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  • Marko, IstvanUCLouvain
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Abstract
The C53-C67 and C53-C65 polyene fragments of amphidinols have been synthesized in an efficient and convergent fashion from sorbic acid in good overall yields (30-31%) by employing a chemoselective cross-metathesis of a Weinreb amide and a Julia-Kocienski olefination as the key steps.
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Cossy, J., Tsuchiya, T., Ferrie, L., Reymond, S., Kreuzer, T., Colobert, F., Jourdain, P., & Marko, I. (2007). Efficient syntheses of the polyene fragments present in amphidinols. Synlett : accounts and rapid communications in synthetic organic chemistry, 14, 2286-2288. https://doi.org/10.1055/s-2007-984910 (Original work published 2007)