A convenient synthesis of p-aminobenzyl-tris(hydroxymethyl)methane as precursor of solid-supported tripodal ligands
(2002) Synthesis : journal of synthetic organic chemistry — n° 1, p. 39-42 (2002)
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- Abstract
- p-Aminobenzyl-tris(hydroxymethyl)methane has been prepared in 5 steps from diethylmalonate and p-nitrobenzyl bromide, with an overall yield of 23%. This compound could be grafted on silica previously derivatized with 3-isocynatopropyltriethoxysilane.
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Duliere, E., & Marchand-Brynaert, J. (2002). A convenient synthesis of p-aminobenzyl-tris(hydroxymethyl)methane as precursor of solid-supported tripodal ligands. Synthesis : journal of synthetic organic chemistry, 1, 39-42. https://doi.org/10.1055/s-2002-19291 (Original work published 2002)