8-(n-methyl-n-tosylamino)bicyclo[4.2.0]octane-7-spiro-2'-oxacyclopropane
(1993) Acta Crystallographica. Section C: Crystal Structure Communications — Vol. 49, p. 561-562 (1993)
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- Abstract
- C17H23NO3S, M(r) = 321.4, monoclinic, P2(1)/c, a = 8.724 (3), b = 12.009 (3), c = 15.780 (4) angstrom, beta = 91.81 (3)-degrees, V = 1652.4 (9) angstrom3, Z = 4, D(x) = 1.29 g CM-3, lambda(Mo Kalpha) = 0.71069 angstrom, mu = 2.08 cm-1, F(000) = 688, T = 291 K, R = 0.071 for 1671 observed reflections. In the four-membered ring the nitrogen substituent is exo; the ring is far from planar, with a dihedral angle about one diagonal of 32 (1)-degrees.
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Feneaudupont, J., Declercq, J.-P., Vanwetswinkel, S., & Genicot, C. (1993). 8-(n-methyl-n-tosylamino)bicyclo[4.2.0]octane-7-spiro-2′-oxacyclopropane. Acta Crystallographica. Section C: Crystal Structure Communications, 49, 561-562. https://doi.org/10.1107/S0108270192008175 (Original work published 1993)