Supported Pd nanoparticles prepared by a modified water-in-oil microemulsion method

Wojcieszak, Robert;Genet, Michel;Eloy, Pierre;Gaigneaux, Eric;Ruiz, Patricio
(2010) Scientific Bases for the Preparation of Heterogeneous Catalysts: 10th International Symposium — Location: Louvain-la-Neuve, Belgium (11.July.2010)

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Authors
  • Wojcieszak, RobertUCLouvain
    Author
  • Genet, MichelUCLouvain
    Author
  • Eloy, PierreUCLouvain
    Author
  • Gaigneaux, Ericorcid-logoUCLouvain
    Author
  • Ruiz, PatricioUCLouvain
    Author
Abstract
Supported Pd nanoparticles (1.6 wt. %) with different diameters were synthesized by the modified water-in-oil microemulsion method using hydrazine as reducing agent. The size of palladium nanoparticles was investigated by varying the nature of the organic surfactant and solvent. The catalysts were characterized by XRD, XPS, ICP, and TEM. Supported palladium nanoparticles (1–8 nm) were obtained. The results confirmed the dependence of the particle size on the nature of organic surfactants. Smaller particles were obtained with organic solvents and anionic surfactants.
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Wojcieszak, R., Genet, M., Eloy, P., Gaigneaux, E., & Ruiz, P. (2010). Supported Pd nanoparticles prepared by a modified water-in-oil microemulsion method. Studies in Surface Science and Catalysis, 175, 789-792. https://doi.org/10.1016/S0167-2991(10)75161-2 (Original work published 2010)